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• Stress Measurement Tool
• Table Top SEM
• Scanning Electron Microscope
• AFM: Veeco Dimension 3100
• AFM: Digital Instruments/Veeco Dimension 3000
• Contact Angle Goniometer
• Spectoscopic Ellipsometer
• Nanospec Reflectometer
• Contact Profilometer
• Microscope with Image Capture
• Four-Point Probes
• High Power Inspection Microscope

NIST CNST NanoFab Equipment
Inspection

Certain commercial equipment, and software, are identified in this documentation to describe the subject adequately. Such identification does not imply recommendation or endorsement by the NIST, nor does it imply that the equipment identified is necessarily the best available for the purpose.


A laser reflection-based surface curvature and stress measurement tool.

Film stress determined by the change in wafer curvature between pre-and post-deposition of film. Curvature is measured by reflected laser beam.

Applications:
  • Film coating stress measurement
  • Stress as a function of time or temperature
  • Stress on multiple films
  • Stress mapping
  • Silicon wafer deformation after grinding
  • Temperature range: -65 to 500 °C
  • Wafer size: 75 to 200mm
  • Speed: 6 seconds/wafer
  • Range: 1 to 4000MPa (1E7-4E10 dy/cm2)
  • Repeatability: 1MPa
Demonstrated use: Stress characterization of silicon nitride membranes; Minimization of stress in multilayer metal films

Toho Technology FLX-2320

Bridges gap between high power optical scope and standard SEM. Ease of use, depth of focus, auto image adjustment and speed (3 min. set-up time)

  • Mag: 20-10,000x
  • Accel. voltage: 15kV
  • Max sample size: 70mm
  • Max sample thick: 20mm
  • Traverse: 15x18mm
  • Measurement markers
Applications:
  • Direct observation of non-conductive samples
  • Stereoscopic observation of surface topography
  • Contrast imaging based on sample atomic number differences
Demonstrated use: MEMs imaging; Inspection of lithography results

Table-top SEM

High performance research grade field emission SEM for imaging

  • Digital system with full function computer control
  • Airlock
  • Pieceparts to 150 mm wafers
  • Secondary and backscattered electron detectors
  • Images structures down to 10 nm in size
  • Resolution: 1.5 nm at 15 keV
  • Magnification: 10x to 1000kx
Applications:
  • Measurement and inspection of nanometer level structures
  • Can accommodate substrates from small pieces to 150 mm wafers
Demonstrated use: Nanolithography inspection, MEMs, Etch cross-sections

Zeiss Ultra-60 FESEM
 

A tool used to characterize the material surface, nanostructures generated by nanofabrication. Nanomanipulation and nanolithography. The tool can take samples up to 200mm in diameter and 12mm in thickness.

  • Contact mode; Tapping mode™, Phase imaging™
  • Electrostatic force microscopy
  • Magnetic force microscopy
  • Nanomanipulation and nanolithography
Applications:
  • Surface characterization for thin films
  • Pattern characterization for lithography structures, magnetic media, CD/DVDs
  • Biomaterials, optics and other samples
  • Nanomanipulation and nanolithography using AFM tip
Demonstrated Use: Nanomagnetic media and Nanofabrication structures characterization

Veeco Dimension 3100
 

A tool used to study the material surface characteristics, check the surface patterns generated by nanofabrication. It can take samples up to 200mm in diameter and 12mm in thickness.

  • Tapping mode; Contact mode; Phase mode
  • Magnetic force microscopy
  • Scanning tunneling microscopy
  • Stepper-motor controlled stage
  • Top view optical microscopy of scanning area
Applications:
  • Surface characterization for thin films
  • Pattern characterization for lithography structures, magnetic media, CD/DVDs
  • Biomaterials, optics and other samples
Demonstrated Use: Nanomagnetic media and Nanofabrication structures characterization

Atomic Force Microscope
 

The FTA32 goniometer provides video-based contact angle and surface tension measurement. Contact angles are measured by fitting a mathematical expression to the shape of a drop and then calculating the slope of the tangent to the drop at the liquid-solid-vapor (LSV) interface line. Computer software drop shape analysis gives contact angle without operator intervention or judgement.

Applications:
  • Contact angle measurement
  • Surface tension calculation
  • Liquid drop shape analysis
Demonstrated Use: Nanoimprint mold treatment; Polymer surface wetting property
Contact Angle Goniometer
 

This system is used to measure thin films properties (thickness and refractive index).

Applications:
  • Thin film characterization
  • Measures thickness, optical constants on single or multi-layer stacks
Demonstrated use: Characterization of Oxides, Resists, Nitrides, Other thin films
Woollam XLS-100
 
Applications: Measures thickness of films such as silicon dioxide, photoresist and nitride Nanospec Reflectometer
 

This system is used to measure step heights by profilometry.

  • Up to 6" wafers
  • Stylus force 1-15mg
  • Tip radius sizes 0.7, 2.5 and 12.5 microns
Applications:
  • Surface characterization of MEMS, semiconductors and other thin/thick films
  • Vertical measurement range of up to 1mm
Demonstrated use: Measurement of Etch rates, Deposition rates, Film growth rates, Surface roughness
Contact Profilometer
 
Optical microscope
with image Capture
Optical Microscope with Image Capture: Nikon
Four-point probe
Four-Point Probes (two units): Jandel RM2
 
Olympus High Power Inspection Microscope
High Power Inspection Microscopes: Olympus
 


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Online: February 2006
Last Updated: September 2008

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